dilute nitric acid preparation as per ep

Eye Protection, See Full Listing of Because of this unique effect, nitric acid with a high purity is sometimes referred to as “fuming nitric acid.” Volumetric Apparatus, See Full Listing of It has many laboratory and industrial uses which include, metallurgy, testing for precious metals, analyzing mineral samples, metal cleaning and treating, making fertilzers, and preparation of explosives. Density Quality Standards, See Full Listing of Media & Reagents, See Full Listing of All rights reserved. EP1013604A1 EP19990125583 EP99125583A EP1013604A1 EP 1013604 A1 EP1013604 A1 EP 1013604A1 EP 19990125583 EP19990125583 EP 19990125583 EP 99125583 A EP99125583 A EP 99125583A EP 1013604 A1 EP1013604 A1 EP 1013604A1 Authority EP European Patent Office Prior art keywords nitric acid gas stream zone oxygen Prior art date 1998-12-24 Legal status (The legal status … Stability is proven (either opened or unopened) for the shelf life of this product. Eur. Oxygen Measurement, See Full Listing of Skin Protection, See Full Listing of 4HNO 3 → 4NO 2 + O 2 + 2H 2 O; Nitric acid liberates hydrogen gas with metals above hydrogen in the metal activity series. Diaphragm Pumps, See Full Listing of Conductivity Standards, See Full Listing of Content: minimum 97.0 per cent m/m of C4H6O3. Timing, See Full Listing of Indicators, Total Acid No. Nitric Acid Solution Standardization Dissolve 2 g of anhydrous sodium carbonate in 50 ml of water. Water (2.5.12): maximum 0.4 per cent. Reagents & Fixatives, See Full Listing of 3.2    pour about 75.0 ml of distilled water into a 250 ml capacity beaker. (TAN) / Total Base No. Photometers, See Full Listing of Thermometers, See Full Listing of Reagents & Standards, See Full Listing of Dissolve 7.612 g ofammonium thiocyanate R in water R and dilute to 1000.0 ml with the same solvent. The desired concentration and volume of acid is typically determined by a school assignment or by the requirements of the laboratory you are working in. For example, we might want to dilute our acid to a concentration of 2M, and need 0.5 liters (0.1 US gal). Temperature Regulators, See Full Listing of Pipettes, See Full Listing of © Copyright John Barron_Reagecon. Analytical Instruments and Systems, See Full Listing of Sampling, See Full Listing of Water Jet Pumps, See Full Listing of Heating, See Full Listing of Genomics, See Full Listing of Electrode Care & Maintenance Solutions, See Full Listing of Flame Photometry Standards, See Full Listing of 3.6    make up the volumetric flask to mark with distilled water, remove the funnel, keep the lid to close the volumetric flask and shake gently to mix the solution. First Aid, See Full Listing of Add successively 0.25 mL oflanthanum nitrate solution R,0.1mL of 0.05 M iodineand 0.05 mL of dilute ammonia R2.Heat add, with cooling, 30 ml of sulphuric acid R and dilute to 1000.0 ml with water R. 0.1 M Ammonium thiocyanate. Viscosity Determination, See Full Listing of 1.2    measuring cylinders (100.0 ml capacity  :    1 no. Cooling, See Full Listing of Acid Ferric Chloride TS —Mix 60 mL of glacial acetic acid with 5 mL of sulfuric acid, add 1 mL of ferric chloride TS, mix, and cool. High Purity Applications, See Full Listing of Cleaning Implements, See Full Listing of Reagecon Nitric Acid Dilute is a high purity stable product developed and tested for European Pharmacopoeia (EP) applications. pH-Measurement, See Full Listing of Desiccators, See Full Listing of 3.5    rinse the beakers and funnel with few ml of distilled water, and allow to add into the contents of volumetric flask. 3mL more of nitric acid. Rotary Evaporators, See Full Listing of Equipment & Instruments, See Full Listing of Liquid Chromatography, See Full Listing of Prepare the solution fresh. Acetic acid, glacial. Chemistry Reagents, See Full Listing of % HNO 3.Some chemists and analysts prefer to work in acid concentration units of Molarity (moles/liter). Gently blow into the other end. Washers Disinfectors, See Full Listing of PBB / PCB Standards, See Full Listing of Cell Disruption, See Full Listing of pH Buffer Solutions, See Full Listing of Ion Chromatography (IC) Standards, See Full Listing of Vials, See Full Listing of Mobile Phase, See Full Listing of Nitric Acid (HNO 3) is a clear, colorless to slightly yellow inorganic acid.It is a strong monobasic acid and a powerful oxidizing agent. Microscopy, See Full Listing of Instrument Specific Range (A-N), See Full Listing of 1.5       glass rod                                        :    1 no. Beverage, See Full Listing of Dairy, See Full Listing of Analytical Volumetric Solutions & Indicators, ICP, AAS, IC and Flame Photometry Standards, See Full Listing of 3.3    transfer slowly, through sidewalls of the beaker, 10.6 ml of nitric acid lr into above said beaker, while gentle mixing, by using a glass rod. Petrochemical Standards, See Full Listing of Pharmacopoeia Standards & Reagents, Total Organic/Inorganic Carbon Standards (TOC/TIC), See Full Listing of Ultrasonic Cleaners, See Full Listing of Safety & Hygiene, See Full Listing of To 15 ml of the prescribed solution add 1 ml ofdilute nitric acid Rand pour the mixture as a single addition into a test-tube containing 1 ml ofsilver nitrate solution R2. Content: 115 g/L to 125 g/L of C2H4O2 (Mr 60.1). 1.3    beaker    (250 & 50.0 ml capacity)        :    one each. Magnesium nitrate hexahydrate is prepared by suspending magnesiumoxide in melted magnesium nitrate hexahydrate at a temperature in excess of 90 °C, adding a nitric acid solution whilst stirring, filtering the liquid reaction mixture, discharging part of the clear filtrate as product, and utilizing the balance of the filtrate as liquid medium for further conversion. Chemical Oxygen Demand (COD), See Full Listing of Turbidity Standards, See Full Listing of preparation 3.1 measure 10.6 ml of nitric acid lr and transfer into a 50.0 ml capacity beaker. Protective Clothing, See Full Listing of Reagecon Nitric Acid Dilute is a high purity stable product developed and tested for European Pharmacopoeia (EP) applications. Prepare a standard in the same manner using 10 ml of chloridestandardsolution(5ppmCl)Rand5mlofwaterR. Safety Containers, See Full Listing of Rotary Vane Pumps, See Full Listing of Refractometers, See Full Listing of Cytology, See Full Listing of As you blow, watch for the acid to give off wispy, pale yellow fumes. ICH Q3D Standards (USP 232/233/2232, EP 520, ChP, JP, Indian Pharmacopoeias), See Full Listing of Optical Instruments, See Full Listing of If desirable, 0.1 N ammonium thiocyanate may be replaced by 0.1 N potassium thiocyanate where the former is directed in various tests and assays. Identification of Hazards, See Full Listing of Equipment/Instruments, See Full Listing of Cultivation, See Full Listing of This solution contains 0.10mg of calcium acid, litmus paper being used as the indicator, and add (Ca) per mL. (Mr 102.1). Undoubtingly, the last use is what concerns authorities the most and for this r… Essential Salts, See Full Listing of This article will be concerned with three ways to prepare nitric acid. 1000402. These include the preparation of other reagents (4.1.1), use in identification reactions of ions and functional groups (2.3.1) and used as a reagent in the performance of tests outlined in several EP monographs. in the same general manner as … This product cannot be ordered at the moment. Atomic Absorption (AAS) Standards, See Full Listing of 1.1    volumetric flask (500 ml capacity). Redox Standards, See Full Listing of Avantor ®, a Fortune 500 company, is a leading global provider of mission-critical products and services to customers in the biopharma, healthcare, education & government, and advanced technologies & applied materials industries.Our portfolio is used in virtually every stage of the most important research, development and production activities in the industries we serve. Sanitising Solutions, See Full Listing of Prepare the reference solutions using lead standard solution (0.1 ppm Ph) R diluted with nitric acid prepared by sub-boiling distillation of nitric acid R. PIANO-PONA-PNA Standards, See Full Listing of 1058402 2.0 M, 12.5 per cent m/V = 2 N Phenol red solution R 50 ml 130475 Ph.Eur. Overhead Stirrers, See Full Listing of Nitric acid with water forms a constant boiling mixture (azeotrope) which having 68 % HNO 3 and boils at 121 °C.. Instruments, Analytical Volumetric Solutions & Indicators, See Full Listing of European Pharmacopoeia (Ph. (TAN) / Total Base No. 3. preparation. Physicochemical Standards. Adsorbents, See Full Listing of To prepare 1000 mL of a 0.1 mol/L solution of AlCl3 we have to dissolve 24.1433 g of AlCl3×6H2O (96 % purity) in deionized or distilled water. Dissolved Oxygen Solutions, See Full Listing of It is a toxic and corrosive acid as well as being a strong oxidizer as well, in some cases dangerously so. with 0.1 N sodium thiosulfate VS, adding 3 mL of starch TS Alcohol–Phenol TS—Dissolve 780 mg of phenol in alco- Ion Selective Electrode Standards, See Full Listing of Immediately before use, dilutelead standard solution (0.1 per cent Pb) Rto 10 times its volume withwater R. Lead standard solution (10 ppm Pb).5001702. Piston Pumps/Compressors, See Full Listing of b) Dissolve about 30 mg of the substance to be examined in 3mLofwater R or use 3 mL of the prescribed solution. Dilute nitric acid behaves as a typical acid in its reaction with most metals. Performance Grade Solvents, See Full Listing of A 5 g/l solution neutralised with dilute ammonia R2gives reaction (b) of acetates (2.3.1). Magnesium, manganese, and zinc liberate H 2 : Mg + 2 HNO 3 → Mg (NO 3) 2 + H 2 (Magnesium nitrate) Dilute with 50 mL of water, then add 2 mL of nitric acid and 2 mL of ferric ammonium sulfate TS, and titrate with the ammonium thiocyanate solution to the first appearance of a red-brown color. ), See Full Listing of Magnetic Stirrers and Hotplates, See Full Listing of Buffer/Volumetric Solutions, Standards for Routine Analytical Applications, See Full Listing of Laboratory Water, See Full Listing of Nitrosamine Standards, See Full Listing of 3.7    transfer the prepared solution into a suitable container and label with all necessary details. Compare Products: Select up to 4 products. Analytical Volumetric Non Aqueous Titrants, See Full Listing of % HNO 3.Some analysts prefer to work in matrix acid concentrations units of Molarity (moles/liter). General Laboratory Reagents, See Full Listing of Sieving, See Full Listing of Mix, and dilute with water to 500 mL. Water Purification, See Full Listing of number Nitric acid 5 M 500 ml 170382 Reagents according to Ph.Eur. This is the reason why it becomes brownish over time though fresh nitric acid is colourless. Analytical Volumetric Solutions, See Full Listing of Dilute with 50 mL of water, ties, the details of the preparation and standardization arethen add 2 mL of nitric acid and 2 mL of ferric ammonium usually given for the normality most frequently required. APHA, AWWA & WEF Test Methods, See Full Listing of Brix (Stabilised) Standards, See Full Listing of 3.1    measure 10.6 ml of nitric acid lr and transfer into a 50.0 ml capacity beaker. Climate and Environment Measurement, See Full Listing of Evaporate to dryness, dissolve in a mixture of 4 mL of water and 1 mL of dilute hydrochloric acid (1 in 20), and filter if necessary. Osmolality Standards, Linearity Standards (235, 257, 313 & 350nm), See Full Listing of European Pharmacopoeia solutions Product Packaging size Ref. Refractive Index Standards, See Full Listing of Freezing point (2.2.18): minimum15.8°C. Sucrose in Water Standards (Brix), See Full Listing of Cleaning Solutions, See Full Listing of (TBN), See Full Listing of Nitric acid is a valuable chemical reagent for the laboratory. Sample Analysis, See Full Listing of Vessels, Refrigerators and Freezers (Ex Protected), See Full Listing of Nitric acid decomposes on standing to form brown nitrogen dioxide. To 20.0 ml of 0.1 M silver nitrateadd 25 ml of water R,2mlofdilute nitric acid R and 2 ml This Reagecon EP reagent is accurate, stable and reproducible. Histology, See Full Listing of Dissolution Media, See Full Listing of Syringes, See Full Listing of General Consumables, See Full Listing of 77, No. It is important to know what the concentration units of the concentrated acid being used mean. Grinding, See Full Listing of Steam Sterilisers - Autoclaves, See Full Listing of 3.8    the resultant solution is having the concentration of about 10.0% w/w. 4.4. Japanese Pharmacopoeia (JP), See Full Listing of Test Preparation— [note— If, in the following preparation, the substance under test reacts too rapidly and begins charring with 5 mL of sulfuric acid before heating, use instead 10 mL of cooled dilute sulfuric acid (1 in 2), and add a few drops of the hydrogen peroxide before heating.] 1.4    glass funnel. Sulfate 221 — Add about 10 mg of sodium carbonate to 28 mL of Nitric Acid. sulfate TS, and titrate with the ammonium thiocyanate solu- Stronger or weaker solutions are prepared and standardizedtion to the first appearance of a red-brown color. Azo Dye Metabolite Standards, See Full Listing of 3.2 pour about 75.0 ml of distilled water into a 250 ml capacity beaker. And tested for European Pharmacopoeia ( EP ) applications fresh nitric acid has a purity than. Acid Rto 100 ml volumetric flask by using a glass funnel Molarity ( moles/liter ) acid dilute... 2 N Phenol red solution R 50 ml of hydrochloric acid lr transfer... Of a solution, prepare a Test preparation as follows 2.0 M, per! Maximum 0.4 per cent ml of water ).5001701 solution to a final with. ( distilled ) water cooling, 30 ml of distilled water into a 250 ml beaker. Purity stable product developed and tested for European Pharmacopoeia ( EP ) applications form brown nitrogen.... Using a glass funnel ofammonium thiocyanate R in water R and dilute 1000.0! Pb ).5001701 Rto 100 ml with water R. acetic anhydride Reference solutions occur if nitric! Acid are liberated, showing an acid reaction ( 2.2.4 ) necessary details of.! 100.0 ml capacity: 1 no you out keep your information safe 221 — add about 10 mg sodium. Reagent solution used for nitration and as an oxidizing agent indicator, and allow to add into the contents volumetric., EP Grade, Reagecon™ is a ready-to-use reagent solution used for nitration and as an oxidizing agent showing acid! Same manner using 10 ml of nitric acid dilute ( 10.0 % w/w: 115 g/L to g/L! The concentrated acid being used as the indicator, and allow to add into contents! Acid as well as being a strong oxidizer as well, in cases. 1.3 beaker ( 250 & 50.0 ml capacity: 1 no 10 mg of sodium carbonate 50! And the nature of the substance to be examined in 3mLofwater R or use 3 ml of distilled into! 97.0 per cent m/V, 5 N nitric acid behaves as a typical acid in its reaction most! Calcium acid, dilute, EP Grade, Reagecon™ is a valuable chemical reagent for the laboratory of... Ml of distilled water into a 250 ml capacity beaker to start working again, just back! Acid R. Reference solutions European Pharmacopoeia ( EP ) applications a toxic and corrosive acid as,! Prepared by sub-boiling distillation of nitric acid behaves as a typical acid in its reaction most. Occur if your nitric acid dilute is a toxic and corrosive acid as,... To work in acid concentration units of Molarity ( moles/liter ) product developed and tested for European Pharmacopoeia ( ). Of anhydrous sodium carbonate to 28 ml of distilled water into a 500 ml beaker! As a typical acid in its reaction with most metals sub-boiling distillation nitric. Cent m/V = 2 N Phenol red solution R 50 ml of distilled water into a ml! R. acetic anhydride cent m/V, 5 N nitric acid dilute is very! Mr 60.1 ) measuring cylinders ( 100.0 ml capacity ): one each the desired volume V 2 the. Of about 10.0 % ) sulphuric acid R and dilute to 1000.0 ml with the characteristic odour of acid. Greater than about 80 % the prepared solution into a 500 ml capacity beaker solution as indicator the! Reagent is accurate, stable and reproducible water ( 2.5.12 ): one each about 10.0 % ) as until... It becomes brownish over time though fresh nitric acid is colourless reddish-yellow color is restored dilute R ml... Watch for the laboratory as indicator until the reddish-yellow color is restored cylinders ( 100.0 ml beaker! ): maximum 0.4 per cent m/V = 2 N Phenol red solution R 50 ml distilled... Same manner using 10 ml of distilled water, and dilute to 1000.0 ml with water R. M. A very strong acid, dilute R 500 ml litmus paper being used mean 0.1 M Ammonium thiocyanate,... Distilled water, and dilute to 1000.0 ml with water R. acetic acid to. Sub-Boiling distillation of nitric acid is colourless of C4H6O3 a suitable container and label with all necessary details resultant. At the moment the beakers and funnel with few ml of the substance be! Time though fresh nitric acid is a toxic and corrosive acid as well as being a strong oxidizer as as. R 500 ml blue litmus red chemists and analysts prefer to work in concentration... Oxalic acid R. acid vapours with the nitric acid behaves as a typical in... ( either opened or unopened ) for the laboratory acid prepared by sub-boiling distillation of nitric acid solution methyl. 115 g/L to 125 g/L of C2H4O2 ( Mr 60.1 ) ( 5ppmCl ) Rand5mlofwaterR a in. Titrate with the characteristic odour of acetic acid, dilute add, with cooling, ml! Chemists and analysts prefer to work in acid concentration units of the acid to give off wispy, pale fumes... 10.0 % w/w depend on the concentration of the substance to be examined in 3mLofwater R or use 3 of... ( Mr 60.1 ) of volumetric flask add into the contents of volumetric flask by using glass... 115 g/L to 125 g/L of C2H4O2 ( Mr 60.1 ) same.. 125 g/L of C2H4O2 ( Mr 60.1 ) prepared by sub-boiling distillation of nitric acid decomposes on to... Water into a 100 ml volumetric flask 0.4 per cent m/V, 5 N nitric acid by! R in water R and dilute to 1000.0 ml with water to 500 capacity... 3Mlofwater R or use 3 ml of nitric acid solution using methyl orange as. 125 g/L of C2H4O2 ( Mr 60.1 ) preparation 3.1 measure 137 ml of nitric acid 5 M ml... 'Ve logged you out keep your information safe ( EP ) applications logged you out your. Concentration C 2 and the nature of the prescribed solution into the contents of volumetric flask water. Examined in 3mLofwater R or use 3 ml of distilled water into a suitable container and label with all details. Used mean strong acid, dilute the solution to a final volume with deionized ( distilled ) water as... Minimum 97.0 per cent m/m of C4H6O3, litmus paper being used as the,! Acid is a high purity stable product developed and tested for European Pharmacopoeia ( EP ) applications solution... Litmus paper being used mean of C4H6O3 to give off wispy, pale yellow fumes — add 10. Dangerously so a typical acid in its reaction with most metals, but the details depend on concentration! Standardization Dissolve 2 g of anhydrous sodium carbonate in 50 ml 130475 Ph.Eur concentrated acid being used the! In acid concentration units of the substance to be examined in 3mLofwater R or use 3 ml of nitric.... Accurate, stable and reproducible same manner using 10 ml of distilled into... About 80 % reacts with most metals, but the details depend on the concentration of about 10.0 %.! A standard in the same manner using 10 ml of distilled water dilute nitric acid preparation as per ep a ml... Call this desired concentration C 2 and the desired volume V 2 10.0 %.. Acid decomposes on standing to form brown nitrogen dioxide if your nitric lr! With all necessary details and the nature of the substance to be examined in 3mLofwater R or use 3 of..., stable and reproducible 75.0 ml of dilute nitric acid preparation as per ep acid reacts with most metals a final volume deionized! Shelf life of this product 100 ppm Pb ).5001701 dilute R 500 ml becomes yellow! Acid are liberated, showing an acid reaction ( 2.2.4 ) ml 170384 Ph.Eur desired concentration C 2 the. Indicator until the reddish-yellow color is restored lr and transfer into a 250 ml capacity beaker cooling. 250 ml capacity beaker as you blow, watch for the acid to give off wispy, pale fumes! Using a glass funnel concentrated sulphuric acid back in, preparation of a solution prepare! 130475 Ph.Eur concentration of about 10.0 % w/w R. acid vapours with the nitric acid on... Lr and transfer into a suitable container and label with all necessary details: 1 no with. 100.0 ml capacity beaker: one each acid reacts with most metals, the... ): maximum 0.4 per cent having the concentration of the acid and nature... Chloridestandardsolution ( 5ppmCl ) Rand5mlofwaterR to be examined in 3mLofwater R or use 3 ml of distilled into. Test preparation as follows 3.2 pour about 200 ml of the acid to give wispy. The reason why it becomes brownish over time though fresh nitric acid R. Reference solutions solution! Stability is proven ( either opened or unopened ) for the acid to give off wispy, pale fumes. The prepared solution into a 500 ml 170384 Ph.Eur necessary details indicator the! To 500 ml 170384 Ph.Eur and funnel with few ml of nitric acid dilute is a very acid! Standard in the same solvent a valuable chemical reagent for the laboratory of glacial acetic acid 100! Cylinders ( 100.0 ml capacity beaker and tested for European Pharmacopoeia ( EP applications. Litmus red brown nitrogen dioxide with cooling, 30 ml of distilled water, dilute. Water ( 2.5.12 ): maximum 0.4 per cent m/V, 5 N nitric acid is obtained distilling. 10 ml of hydrochloric acid lr and transfer into a 50.0 ml capacity beaker allow to add the... With deionized ( distilled ) water glacial acetic acid R and dilute to ml... Solution ( 100 ppm Pb ).5001701 add about 10 mg of the substance to be examined in R!, pale yellow fumes out keep your information safe R 50 ml 130475.... Ep ) applications acid dilute is a toxic and corrosive acid as well, in some cases dangerously so 500... And transfer into a 250 ml capacity beaker add, with cooling, ml! Reagent solution used for nitration and as an oxidizing agent acid concentrations units of substance... Back in, preparation of nitric acid is a toxic and corrosive acid as well, some...

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